| TCI产品编码 : | B1676 | ||||||||||||||
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| 库存情况 : |
2012年02月09号上午06点的情况 *2012年4月前，中国库存将暂时显示上海仓库和天津仓库的库存总和。 |
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| 纯度 / 分析方法 : | >98.0%(T) | ||||||||||||||
| 保存温度 : | |||||||||||||||
| 分子式 / 分子量 : | C4H6Cl2N2Pd=259.43 | ||||||||||||||
| CAS编码 : | 14592-56-4 | ||||||||||||||
| 相关CAS编码 : | |||||||||||||||
| MDL编码 : | MFCD00013122 | ||||||||||||||
| 监管条件代码 : | |||||||||||||||
| 国内危险化学品编码 : | |||||||||||||||
Synthesis of Oxindoles Typical Procedure: To a dried screw-cap vial is added anilide (0.3 mmol), AgOCOCF3 (132.5 mg, 0.6 mmol), (CH3CN)2PdCl2 (3.5 mg, 0.015 mmol) and chlorobenzene. The reaction mixture is stirred at 100-120 °C for 3-12 h in a pre-heated oil bath. After cooling to room temperature, the reaction is diluted with EtOAc and filtered with a glass filter. The filtrate is washed with 5% aqueous NaHCO3 and brine. The extract is dried over MgSO4 and concentrated in vacuo. The crude is purified by preparative TLC. |
| F & F : | 14, 35 |
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| UN编号 : | 3439 |
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| Class : | 6.1 |
| PG : | III |
| TCI产品学术记录 : | |
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| 相关分类 : |
Structure of Chemicals
Classes of Metal Compounds
Transition Metal Compounds
Pd (Palladium) Compounds
Synthetic Organic Chemistry Catalysts for Organic Synthesis Homogeneous Catalysts Metal Complexes Synthetic Organic Chemistry Catalysts for Organic Synthesis Homogeneous Catalysts Palladium Synthetic Organic Chemistry Suzuki-Miyaura Cross-coupling Palladium Catalyst (for Suzuki-Miyaura Cross-coupling) |